List
of Experiments
Chemistry 315
FALL,
2009
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Lab
Text: D.L. Pavia, et al., Introduction
to Organic Laboratory Techniques, 2nd Edition .
Lab
Manual:
S.W. Slayden and W.M. Stalick, Organic Chemistry Laboratory
Manual, 2005.
The Pavia, Lampman, Kriz & Engel lab text reading assignment
for each week appears below. The procedures for most experiments
are in the Lab Manual (although not necessarily in the order
in which they are performed). If a procedure appears in both
the text and the manual, the procedure in the manual will
be used.
Chem 313 lecture is a pre- or
co-requisite for Chem 315 lab. The last day
to add is Sept. 15. If you drop Chem 313, you must
also drop Chem 315 or the department will drop you. The drop deadline is Oct. 2.
Lab classes
do not meet during the weeks of Sept. 7, Oct. 12, and Nov.
23.
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| Week
of: |
Experiment
Title |
Lab
Text |
| Aug.
31 |
Introduction,
Safety, Check-in |
pp.
2-5; Technique 1; 3.9 |
| Sept.
14 |
Melting
Point and Refractive Index Experiment |
Technique 2;
24;
9.1-9.5,
9.7-9.9 |
| Sept.
21 |
Crystallization
|
Technique 11 (pp. 679-684, 687-688, 694);
6.2,
6.3 |
| Sept.
28
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Infrared,
Mass Spec.,
and UltraViolet Spectroscopy
Spectroscopy Problem Set |
Solomons & Fryle Sec. 2.16; 9.13-9.17; 13.9
Technique 25.9-25.14; 28
Unknown List (replaces Appendix 3) |
| Oct.
5 |
Identification of an Unknown (IR continued)
Simple Distillation to Determine Boiling Point |
Technique 3.3-3.8; 6.1; 13.1; 14.1-14.3;
25.-25.2, 25.4, 25.7 |
| Oct.
19 |
Gas
Chromatography: Acetates |
Technique 22.1-22.13; Manual p. 45 |
| Oct.
26 |
Distillation
of a Mixture
|
Technique 15.1-15.6 |
| Nov. 2 |
Gas
Chromatography: Distillate |
Manual p. 39 |
| Nov. 9 |
Synthesis
of t-BuCl |
pp.
187-188; Technique 12.1-12.4, 12.8-12.10 |
Nov.
16 &
Nov. 30 |
Qualitative
Organic Analysis:
alkanes, alkenes, alkynes, aromatics,
alkyl & aryl halides, alcohols |
Experiment
55:
pp. 468-479, 480-482,
486-491, 507-511 |
| Dec. 7 |
Lab
Final Exam and Checkout |
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For
more information or materials for your particular lab section,
go back and click on your professor's
name.
The
URL for this page is http://classweb.gmu.edu/chemlab/315/315expts.htm
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