List of
Experiments
Chemistry 315
Spring, 2012
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Lab Text:
D.L. Pavia, et al., Introduction to Organic Laboratory Techniques:
A Small Scale Approach (GMU edition).
Lab Manual:
S. W. Slayden, R. J. Roth and W. M. Stalick, Organic Chemistry
Laboratory Manual, 2011.
Lecture Text: Solomons & Fryle, Organic Chemistry, 10th Edition.
The Pavia, Lampman, Kriz & Engel lab
text reading assignment for each lab meeting appears below in boldface.
The procedures for most experiments are in the Lab Manual. If a procedure
appears in both the text and the manual, the procedure in the manual will
be used.
Chem 313 lecture is a pre- or co-requisite for Chem 315 lab.
The last day to add is Jan.
31. If you drop or withdraw from Chem
313, you must also drop/withdraw from Chem 315.
The last day to drop is Feb
24.
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Week Beginning
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Experiment Title
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Reading Assignment
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Jan 23
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Introduction, Safety, Check-in
Citing Information in the Laboratory
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Technique 1; 2; 3
Manual pp. 1-20
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30
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Melting Point and Refractive Index
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Techniques 9
(9.1-9.5, 9.7-9.9) ; 24
Manual pp. 23-28
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Feb 6
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Crystallization
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Techniques 6 (6.2,
6.5, 6.6, 6.9); 11 (11.1-11.3A,C-D, 11.5, 11.6, 11.8-11.10)
Manual pp. 29-32
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13
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Infrared, Mass Spec.,
and UltraViolet Spectroscopy
Spectroscopy Problem Set
[pdf or doc]
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Solomons & Fryle Sec. 2.15-2.16; 9.13-9.17;13.9
and/or
Techniques 25 (25.9-25.14); 28
Manual pp. 33-44
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20
27
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Simple Distillation to Determine Boiling Point. Identification
of an Unknown (IR continued)
Isolation of Caffeine from Tea Leaves
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Techniques 3
(3.3-3.8); 13.1; 14 (14.1-14.3); 25 (25.1, 25.2, 25.4, 25.7)
Experiment: pp. 85-89
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March 5
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Gas Chromatography: Acetates
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Technique 22
(22.1-22.7, 22.9-22.10, 22.12)
Manual pp. 45-48
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12
19
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Spring Break
Simple and Fractional Distillation
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No
Classes
Technique
15.1-15.6
Manual pp. 49-53
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26
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Gas Chromatography: Distillate
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Technique 22
(22.8, 22.11, 22.13, 22.14)
Manual p. 55-56
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April 2
9
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Synthesis of tert-BuCl
Synthesis of Cyclohexene
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Technique 12 (12.1-12.4, 12.8-12.10);
Experiment 21: pp. 172-174
Manual pp. 57-59
Solomons & Fryle pp. 297-302
Experiment: pp. 179-183
Manual pp. 61-62
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16
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Qualitative Organic Analysis:
alkanes, alkenes, alkynes, aromatics,
alkyl & aryl halides, alcohols
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Experiment 55: pp. 446-461, 464-468, 483-487
Manual pp. 65-69
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23
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Qualitative Analysis, continued
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30
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Lab Check-out and Final Exam
CHEM 315 Report Forms
The URL of the lab website is
http://classweb.gmu.edu/chemlab/
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